The Heterogenation Of Iron-Carbonyl Thiourea Complex Onto Rice Husk Silica And Its Catalytic Oxidation Of Limonene With Hydrogen Peroxide

• Main Author: Ameram, Nadiah
• Format: Thesis
• Language: English
• Published: 2017
• Subjects: QD1-999 Chemistry
• Online Access: http://eprints.usm.my/39214/

Tiga ligan tiourea yang baru 2-metil-N-[(2-piridina-2-il-etil)karbamotiol] benzamida, O2; 4-metil-N-[(4-metilpiridina-2-il)karbamotiol]benzamida, P1; dan 4-metil-N-[(2-piridina-2-il-etil)karbamotiol]benzamida, P2 telah disintesis dan diciri- kan melalui pelbagai teknik spektral dan analitikal seperti NMR (1H and 13C), spektroskopi FTIR dan analisis unsur Three new thiourea ligands (2-methyl-N-[(2-pyridine-2-yl-ethyl)carbamothioyl] benzamide, O2; 4-methyl-N-[(4-methylpyridin-2-yl) carbamothioyl]benzamide, P1; and 4-methyl-N-[(2-pyridine-2-yl-ethyl)carbamothioyl]benzamide, P2) were synthesized and characterized by various spectroscopic and analytical techniques viz., NMR (1H and 13C), FTIR and elemental analysis