Preparation And Characterization Of Recycled Carbon/Fibercarbon Nanotube Reinforced Epoxy Composites

The usage of carbon fiber reinforced polymers (CFRP) has been growing at a substantial rate that leads to the increasing amount of waste generated from end-of-life components and manufacturing scrap. Recognizing the hazardous waste that would be harmful to the human health as well as the environment...

وصف كامل

التفاصيل البيبلوغرافية
المؤلف الرئيسي: Law, Mei Lin
التنسيق: أطروحة
اللغة:الإنجليزية
الإنجليزية
منشور في: UTeM 2016
الموضوعات:
الوصول للمادة أونلاين:http://eprints.utem.edu.my/id/eprint/18574/
https://plh.utem.edu.my/cgi-bin/koha/opac-detail.pl?biblionumber=101060
HF5351.M34 2016
Abstract Abstract here
_version_ 1855619632482746368
author Law, Mei Lin
author_facet Law, Mei Lin
author_sort Law, Mei Lin
description The usage of carbon fiber reinforced polymers (CFRP) has been growing at a substantial rate that leads to the increasing amount of waste generated from end-of-life components and manufacturing scrap. Recognizing the hazardous waste that would be harmful to the human health as well as the environment, this has poses the need to recycle the waste. This report presents the research of compression and wear behaviour of as-received as well as treated rCF and carbon nanotube (CNT) reinforced epoxy composites. The rCF derived from mechanically recycled CFRP composite woven prepreg waste - materials impregnated with epoxy resin is of low value commodity. Therefore, cyclic cryogenic treatment is introduced to produce valuable product of rCF. The objectives of this study were to investigate the effect of cyclic cryogenic treatment on the recycled carbon fiber as well as to study the performance of the as-received rCF reinforced epoxy (EP/rCF-AR), treated rCF reinforced epoxy (EP/rCF-T) and carbon nanotube reinforced treated rCF and epoxy (EP/rCF-T/CNT) composites. The composites’ samples were fabricated using vacuum casting technique. The samples were then subjected to physical, compression and tribological testing. In addition, microscopy examinations were carried out to observe and to analyse the morphology of the worn surfaces. It was found that at 25 cycles of cryogenic treatment, the epoxy resin on the surface of rCF is nearly absent, indicating the effective removal of epoxy resin due to the mismatches in thermal expansion between the interface bonding of rCF/epoxy. Based on the compression and wear test analysis, it was observed that the reinforcement effect of rCF-T has improved the compressive strength (4.09 %) and significantly enhanced the wear resistance (32.2 % at 1.0 m/s and 16 N) of epoxy composites as compared to rCF-AR which may attribute to the improved adhesion between the treated rCFs and epoxy matrix. Moreover, further improvement can be seen in EP/rCF-T/CNT as compared to EP/rCF-T for compressive strength (6.18 %) and wear resistance (16.4 % at 1.0 m/s and 16 N). This is because the addition of nano-size CNT in the composite has enhanced the local stress transferred by the matrix and the good reinforcing capability of CNT promotes better adhesion at the polymer matrix interface. From the study, it was clearly shown that the treated rCF was effective in improving the properties of the epoxy composites. Therefore, the treated rCF are valuable product worth to be considered as reinforcements in the composite materials. In addition, nanofillers serve as matrix reinforcement even at low filler content.
format Thesis
id utem-18574
institution Universiti Teknikal Malaysia Melaka
language English
English
publishDate 2016
publisher UTeM
record_format EPrints
record_pdf Restricted
spelling utem-185742021-10-10T16:39:31Z http://eprints.utem.edu.my/id/eprint/18574/ Preparation And Characterization Of Recycled Carbon/Fibercarbon Nanotube Reinforced Epoxy Composites Law, Mei Lin T Technology (General) TA Engineering (General). Civil engineering (General) The usage of carbon fiber reinforced polymers (CFRP) has been growing at a substantial rate that leads to the increasing amount of waste generated from end-of-life components and manufacturing scrap. Recognizing the hazardous waste that would be harmful to the human health as well as the environment, this has poses the need to recycle the waste. This report presents the research of compression and wear behaviour of as-received as well as treated rCF and carbon nanotube (CNT) reinforced epoxy composites. The rCF derived from mechanically recycled CFRP composite woven prepreg waste - materials impregnated with epoxy resin is of low value commodity. Therefore, cyclic cryogenic treatment is introduced to produce valuable product of rCF. The objectives of this study were to investigate the effect of cyclic cryogenic treatment on the recycled carbon fiber as well as to study the performance of the as-received rCF reinforced epoxy (EP/rCF-AR), treated rCF reinforced epoxy (EP/rCF-T) and carbon nanotube reinforced treated rCF and epoxy (EP/rCF-T/CNT) composites. The composites’ samples were fabricated using vacuum casting technique. The samples were then subjected to physical, compression and tribological testing. In addition, microscopy examinations were carried out to observe and to analyse the morphology of the worn surfaces. It was found that at 25 cycles of cryogenic treatment, the epoxy resin on the surface of rCF is nearly absent, indicating the effective removal of epoxy resin due to the mismatches in thermal expansion between the interface bonding of rCF/epoxy. Based on the compression and wear test analysis, it was observed that the reinforcement effect of rCF-T has improved the compressive strength (4.09 %) and significantly enhanced the wear resistance (32.2 % at 1.0 m/s and 16 N) of epoxy composites as compared to rCF-AR which may attribute to the improved adhesion between the treated rCFs and epoxy matrix. Moreover, further improvement can be seen in EP/rCF-T/CNT as compared to EP/rCF-T for compressive strength (6.18 %) and wear resistance (16.4 % at 1.0 m/s and 16 N). This is because the addition of nano-size CNT in the composite has enhanced the local stress transferred by the matrix and the good reinforcing capability of CNT promotes better adhesion at the polymer matrix interface. From the study, it was clearly shown that the treated rCF was effective in improving the properties of the epoxy composites. Therefore, the treated rCF are valuable product worth to be considered as reinforcements in the composite materials. In addition, nanofillers serve as matrix reinforcement even at low filler content. UTeM 2016 Thesis NonPeerReviewed text en http://eprints.utem.edu.my/id/eprint/18574/1/Preparation%20And%20Characterization%20Of%20Recycled%20Carbon%20Fibercarbon%20Nanotube%20Reinforced%20Epoxy%20Composites%2024%20Pages.pdf text en http://eprints.utem.edu.my/id/eprint/18574/2/Preparation%20And%20Characterization%20Of%20Recycled%20Carbon%20Fiber%20Carbon%20Nanotube%20Reinforced%20Epoxy%20Composites.pdf Law, Mei Lin (2016) Preparation And Characterization Of Recycled Carbon/Fibercarbon Nanotube Reinforced Epoxy Composites. Masters thesis, Universiti Teknikal Malaysia Melaka. https://plh.utem.edu.my/cgi-bin/koha/opac-detail.pl?biblionumber=101060 HF5351.M34 2016
spellingShingle T Technology (General)
TA Engineering (General). Civil engineering (General)
Law, Mei Lin
Preparation And Characterization Of Recycled Carbon/Fibercarbon Nanotube Reinforced Epoxy Composites
thesis_level Master
title Preparation And Characterization Of Recycled Carbon/Fibercarbon Nanotube Reinforced Epoxy Composites
title_full Preparation And Characterization Of Recycled Carbon/Fibercarbon Nanotube Reinforced Epoxy Composites
title_fullStr Preparation And Characterization Of Recycled Carbon/Fibercarbon Nanotube Reinforced Epoxy Composites
title_full_unstemmed Preparation And Characterization Of Recycled Carbon/Fibercarbon Nanotube Reinforced Epoxy Composites
title_short Preparation And Characterization Of Recycled Carbon/Fibercarbon Nanotube Reinforced Epoxy Composites
title_sort preparation and characterization of recycled carbon fibercarbon nanotube reinforced epoxy composites
topic T Technology (General)
TA Engineering (General). Civil engineering (General)
url http://eprints.utem.edu.my/id/eprint/18574/
https://plh.utem.edu.my/cgi-bin/koha/opac-detail.pl?biblionumber=101060
HF5351.M34 2016
work_keys_str_mv AT lawmeilin preparationandcharacterizationofrecycledcarbonfibercarbonnanotubereinforcedepoxycomposites