3D/4D printing of photopolymer uv resin consisting Polycaprolactone (PCL) as healing agent

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Bibliographic Details
Main Author: Lee, Kok Wai
Other Authors: Habibah Ghazali, supervisor
Format: Bachelor thesis
Language:ENG
Published: Universiti Teknologi Malaysia 2025
Subjects:
Online Access:https://utmik.utm.my/handle/123456789/41732
Abstract Abstract here
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author Lee, Kok Wai
author2 Habibah Ghazali, supervisor
author_facet Habibah Ghazali, supervisor
Lee, Kok Wai
author_sort Lee, Kok Wai
description Not available
format Bachelor thesis
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institution Universiti Teknologi Malaysia
language ENG
publishDate 2025
publisher Universiti Teknologi Malaysia
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record_pdf Abstract
spelling utm-123456789-417322025-08-21T04:08:48Z 3D/4D printing of photopolymer uv resin consisting Polycaprolactone (PCL) as healing agent Lee, Kok Wai Habibah Ghazali, supervisor Mechanical engineering Not available 3D/4D printing is an active additive manufacturing research topic because it is advantageous to many areas such as manufacturing and biomedical sectors. Polymer blends are utilised as ‘inks’ to make 3D structures. Acrylonitrile butadiene styrene (ABS) photopolymer UV resin is suitable to make polymer blends because it has good mechanical properties. On the other hand, polycaprolactone (PCL) is a thermoplastic polyester which grants a polymer resin both healing and shape memory abilities when blended together. Such abilities are important to improve the durability of ABS photopolymer UV resin. However, it is not known whether PCL is able to imbue ABS the abilities because no work is done to address the issues. The objectives of this project are to investigate the printability of the PCL/ABS photopolymer UV resin blend and investigate the thermal activated healing and shape memory abilities of the PCL/ABS resin blend. This project aims to show that blending ABS with PCL enables the 3D specimens printed using the resin blend to exhibit thermal activated healing and shape memory abilities. The resin blend is synthesised to fulfil the printing requirements of digital light processing (DLP). Synthesis is done by melt-mixing 100g of ABS photopolymer UV resin and 5g of PCL pellets using a magnetic stirrer at 200rpm and 90°C for three hours. Acetone is added during the melt-mixing process. The resulting homogenous resin blend contains 5 wt% PCL. Next, 3D specimens are printed using the resin blend. On top of that, 3D control specimens are also printed using ABS photopolymer UV resin. Thermal characterisation of the two classes of specimens is conducted via differential scanning calorimetry (DSC). Theoretical study on past research findings of PCL-enriched polymer blends is performed which focuses on three aspects namely thermal activated healing ability, healing mechanism and thermal activated shape memory ability. This is done to produce reasonable theoretical predictions regarding the three aforementioned aspects of the PCL/ABS resin blend. The 3D specimens printed using the PCL/ABS resin blend have imperfections namely deformation and delamination. They are a result of PCL-modification of ABS which causes the latter being unable to fully support shape formation during printing and experimental errors occurred during film sheet set-up and specimen removal. Based on the DSC results, the glass transition temperatures of the 3D control specimens and 3D PCL-enriched specimens are 110.40? and 86.90? respectively. The dissimilar values indicate that both PCL and ABS phases are completely miscible in the resin blend. Besides, four theoretical predictions are made. Firstly, the PCL/ABS resin blend exhibits thermal activated healing ability because PCL acts as the healing agent. Secondly, the PCL/ABS resin blend does not possess the bricks/mortar morphology due to its low PCL content of 5 wt%. Thirdly, the healing mechanism of the PCL/ABS resin blend is due to the “bleeding” behaviour of the molten PCL phase. Lastly, the PCL/ABS resin blend exhibits thermal activated shape memory ability due to PCL’s shape memory functionality. The experimental findings and theoretical predictions obtained indicate the PCL/ABS photopolymer UV resin blend has the potential to be utilised by 3D/4D printing. fahmimoksen UTM 135 p. Project Paper (Bachelor of Engineering (Mechanical-Materials)) - Universiti Teknologi Malaysia, 2021 2025-03-10T03:03:35Z 2025-03-10T03:03:35Z 2021 Bachelor thesis https://utmik.utm.my/handle/123456789/41732 vital:154067 valet-20231030-102415 ENG Closed Access UTM Complete Unpublished Completion application/pdf Universiti Teknologi Malaysia
spellingShingle Mechanical engineering
Lee, Kok Wai
3D/4D printing of photopolymer uv resin consisting Polycaprolactone (PCL) as healing agent
title 3D/4D printing of photopolymer uv resin consisting Polycaprolactone (PCL) as healing agent
title_full 3D/4D printing of photopolymer uv resin consisting Polycaprolactone (PCL) as healing agent
title_fullStr 3D/4D printing of photopolymer uv resin consisting Polycaprolactone (PCL) as healing agent
title_full_unstemmed 3D/4D printing of photopolymer uv resin consisting Polycaprolactone (PCL) as healing agent
title_short 3D/4D printing of photopolymer uv resin consisting Polycaprolactone (PCL) as healing agent
title_sort 3d 4d printing of photopolymer uv resin consisting polycaprolactone pcl as healing agent
topic Mechanical engineering
url https://utmik.utm.my/handle/123456789/41732
work_keys_str_mv AT leekokwai 3d4dprintingofphotopolymeruvresinconsistingpolycaprolactonepclashealingagent