Physical, structural and optical properties of erbium doped tellurite glass with copper oxide nanoparticles embedment

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التفاصيل البيبلوغرافية
المؤلف الرئيسي: Nur E�zzati Nabilah Syaqilah Abdul Hamid
مؤلفون آخرون: Ezza Syuhada Sazali, supervisor
التنسيق: Master's thesis
اللغة:الإنجليزية
منشور في: Universiti Teknologi Malaysia 2025
الموضوعات:
الوصول للمادة أونلاين:https://utmik.utm.my/handle/123456789/46779
Abstract Abstract here
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author Nur E�zzati Nabilah Syaqilah Abdul Hamid
author2 Ezza Syuhada Sazali, supervisor
author_facet Ezza Syuhada Sazali, supervisor
Nur E�zzati Nabilah Syaqilah Abdul Hamid
author_sort Nur E�zzati Nabilah Syaqilah Abdul Hamid
description Also available in printed version
format Master's thesis
id utm-123456789-46779
institution Universiti Teknologi Malaysia
language English
publishDate 2025
publisher Universiti Teknologi Malaysia
record_format dspace
record_pdf Abstract
spelling utm-123456789-467792025-08-21T12:09:40Z Physical, structural and optical properties of erbium doped tellurite glass with copper oxide nanoparticles embedment Nur E�zzati Nabilah Syaqilah Abdul Hamid Ezza Syuhada Sazali, supervisor Science Also available in printed version Two series of glass with composition of (70�x)TeO2 � 10ZnO � 10MgO � 10 Na2O � (x)Er2O3 where 0.0 =x = 2.0 mol% and (69�y)TeO2 � 10ZnO � 10MgO � 10Na2O � 1Er2O3 � (y)CuO where 0.05 = y = 1.50 mol% are prepared using melt quenching technique. The physical properties are measured in terms of glass density, ionic packing density and molar volume while the glass hardness is determined by using Vickers Microhardness. The amorphous nature of the glass is determined by X-ray Diffractometer (XRD). The occurrence of copper oxide nanoparticles (CuO NPs) is verified by using High-Resolution Transmission Electron Microscopy (HRTEM). The structural and optical properties are characterized by using Fourier Transform Infrared (FTIR), UV-Visible-NIR spectrophotometer and Photoluminescence (PL) spectrometer, respectively. The glass density, molar volume, ionic packing density and hardness are found in the range of (4.799 � 4.951) g cm-3, (26.575 � 27.202) cm3 mol-1, (0.457 � 0.467) and (235 � 349), respectively. It is found that all glasses are amorphous in nature while the presence of CuO NPs with lattice spacing 0.23 nm at (111) plane is verified by HRTEM analysis. FTIR spectrum exhibited three major bands which are attributed to Te � O � Te, TeO4 and TeO3 in the range of 400 � 4000 cm-1. Meanwhile, UV-Visible-NIR spectra reveal nine absorption peaks centered at about 407, 449, 488, 522, 545, 652, 799, 976 and 1530 nm originating from 4I15/2 to 2H9/2, 4F5/2, 4F7/2, 2H11/2, 4S3/2, 4F9/2, 4I9/2, 4I11/2 and 4I13/2 transitions respectively. Down-conversion emission spectra under 380 nm excitations shows four peaks centered at about 408, 530, 550, and 660 nm allocated to 4F3/2 ? 4I15/2, 2H11/2 ? 4I15/2, 4S3/2 ? 4I15/2 and 4F9/2 ? 4I15/2 transition. Meanwhile, up-conversion emission spectra under 980 nm excitations shows peaks three centered at about 530, 550, and 660 nm allocated to 2H11/2 ? 4I15/2, 4S3/2 ? 4I15/2 and 4F9/2 ? 4I15/2 transition fahmimoksen UTM 116 p. Thesis (Sarjana Sains (Fizik)) - Universiti Teknologi Malaysia, 2018 2025-03-12T05:17:31Z 2025-03-12T05:17:31Z 2018 Master's thesis https://utmik.utm.my/handle/123456789/46779 vital:124945 valet-20190530-112546 ENG Closed Access UTM Complete Unpublished Completion application/pdf Universiti Teknologi Malaysia
spellingShingle Science
Nur E�zzati Nabilah Syaqilah Abdul Hamid
Physical, structural and optical properties of erbium doped tellurite glass with copper oxide nanoparticles embedment
thesis_level Master
title Physical, structural and optical properties of erbium doped tellurite glass with copper oxide nanoparticles embedment
title_full Physical, structural and optical properties of erbium doped tellurite glass with copper oxide nanoparticles embedment
title_fullStr Physical, structural and optical properties of erbium doped tellurite glass with copper oxide nanoparticles embedment
title_full_unstemmed Physical, structural and optical properties of erbium doped tellurite glass with copper oxide nanoparticles embedment
title_short Physical, structural and optical properties of erbium doped tellurite glass with copper oxide nanoparticles embedment
title_sort physical structural and optical properties of erbium doped tellurite glass with copper oxide nanoparticles embedment
topic Science
url https://utmik.utm.my/handle/123456789/46779
work_keys_str_mv AT nurezzatinabilahsyaqilahabdulhamid physicalstructuralandopticalpropertiesoferbiumdopedtelluriteglasswithcopperoxidenanoparticlesembedment